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- Numerical Thermal Analysis of a T Jump System Used for Studying Polymer BehaviourPublication . Gomes, S.; Pascoal-Faria, P.; Mitchell, G. R.; Gkourmpis, T.; Youngs, T.The processing of polymers is highly complex. The study of their crystallisation assumes an important role and needs to be carefully detailed. Scattering experiments can be used to study polymer molecular organisation. However these procedures are still very multifaceted leading to the need for planning all the details in the experiments that are to be performed. This manuscript presents a finite element model developed to study the temperature variation of a T Jump System, which has been used for studying polymer behaviour with the NIMROD instrument at the ISIS Neutron and Muon Source, UK. Results show that the variation across the sample was 2ºC at a maximum temperature of 70ºC and 1ºC at a maximum temperature of 50ºC.
- Measuring in-situ X-ray scattering of natural rubber biaxial deformation: A new equipment for polymer studiesPublication . Silva, Daniel P. da; Lamolinara, Barbara; Costa, André; Gameiro, Fábio; Pascoal-Faria, Paula; Mateus, Artur; Martinez, Juan Carlos; Phinyocheep, Pranee; Amornsakchai, Taweechai; Mitchell, Geoffrey R.Understanding biaxial deformation is essential for a more realistic evaluation of rubber elasticity compared to the more usual uniaxial deformation. To study crystallisation occurring during biaxial deformation of natural rubber films, a new simple equipment has been designed and assembled. The equipment, mounted in the beamline of ALBA synchrotron light source facility, allowed the in-situ measurement of X-ray scattering of natural rubber during biaxial deformation. This work provides, for the first time, quantitative information on crystallisation during biaxial extension.