Browsing by Author "Franco, M. C."
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- Cork Plastic Composite Optimization for 3D Printing ApplicationsPublication . Brites, F.; Malça, C.; Gaspar, F.; Horta, J. F.; Franco, M. C.; Biscaia, S.; Mateus, A.Among natural fillers, cork has been acknowledged as a suitable alternative of other cellular materials that are widely employed in engineering applications due to their low conductivity to heat, noise and vibration, high abrasion resistance and flexibility, high compressibility ratio, among other characteristics [1]. The eco-friendly features of natural fillers based composites make them a very promising and sustainable solution to large markets mainly if additive manufacturing technologies, such as 3D printing, are used [2]. Through 3D printers, engineers, designers and architects can create design and decor products with a free complexity of geometry. In this research work, plastic matrices of HDPE – obtained from conventional suppliers – were reinforced with different ratios of cork waste and natural cork powders – obtained from cork transformation industries – to find the optimum mixture for 3D printing. The effects of cork powders content in the plastic on the morphological, physical and mechanical properties of the composites were investigated through the density, optical microscopy, wettability, thermal analysis and tensile testing. Cork-based composites were processed by an extrusion system, and the mixture of polymer, adhesive and fillers is discussed. The results show that the addition of pure cork and cork waste can be processed with polymers such as HDPE, having adequate physical and mechanical properties.
- Micro Computed Tomography Detects Changes in Liver Density in Control and in Prediabetes RatsPublication . Fonseca, A. R.; Franco, M. C.; Sacramento, J.; Melo, B.; Conde, S.V.; Guarino, M. P.Fatty liver disease is an early event in the development of insulin resistance that predicts the presence and progression of the metabolic syndrome. In humans, fatty liver diagnosis is usually performed by imaging techniques based on ultrasound, computed tomography and magnetic resonance. Rodent models are often used in metabolic research allowing access to tissue biopsies however, studies describing ex vivo computed tomography of biological samples are scarce. X-ray Micro Computed Tomography (Micro-CT) is an imaging technique that reveals the internal structure of materials in great detail, also allowing a quantitative analysis of properties such as density measured as arbitrary Hounsfield Units (HU). Herein, we tested the hypothesis that Micro CT detects changes in liver tomographic density induced by metabolic diseases and its reversal upon therapeutic surgical intervention. Two groups of male Wistar rats were used: a group submitted to a hypercaloric diet for 14 weeks to induce prediabetes and the control group submitted to a standard diet). The animals were randomly submitted to a surgical treatment and maintained on their respective diets after the procedure for 11 more weeks. Liver and adipose tissues samples were excised and samples were scanned using a compact X-ray micro-CT scanner. The projection images obtained were analyzed and reconstructed and values of HU density were calculated after calibration for all samples. Results showed that liver density was lower in prediabetes rats (74.8±5.87 HU) than in control animals (97.2±6.3 HU), p<0.05. Liver density was not affected by surgical treatment in control animals however, in prediabetes animals, the surgical therapy restored liver density to control values. Visceral fat density was significantly lower than hepatic density, as expected and was affected, neither by the disease condition nor by the surgical treatment. We concluded that micro-CT detects metabolic disease-induced changes in liver density, but not in visceral adipose tissue density in biopsy samples ex vivo. Changes in hepatic density, assessed by micro-CT, correlate with disease state and with therapeutic interventions.
- The Use of Polypropylene and High-Density Polyethylene on Cork Plastic Composites for Large Scale 3D PrintingPublication . Brites, Fernando; Malça, Cândida; Gaspar, F.; Horta, J. F.; Franco, M. C.; Biscaia, S.; Mateus, A.This work focuses on studying the possibility of 3D printing of composite materials composed by cork and a polymer matrix (CPC). Initially the cork was mixed with two types of polymers (HDPE and PP) in different proportions and later processed using extrusion and injection. The composites were tested to study the physical, chemical and mechanical properties. The material was then tested on a large-scale 3D printer to study its feasibility and the ability to produce new products through 3D printing. Attention was focused on the use of pure cork, varying the concentration of cork and coupling agent in thermoplastic matrix composites of PP and HDPE. It was demonstrated that the increase of 5wt.% of coupling agent in the two types of polymers significantly improved the mechanical properties and adhesion between the phases but the increase in cork concentration decreased mechanical properties and crystallinity. The CPCs with PP showed to have better mechanical properties, better aesthetic and internal structural quality, and easier processability than those with HDPE matrix. Nevertheless, the HDPE CPCs showed a high degree of crystallization. Concerning 3D printing, it was demonstrated the possibility of making new products based on natural cork fibers, showing promising results, although additional research is still needed to optimize the process.